Multidimensional Spectroscopy of Polymers. Vibrational, NMR, by Marek W. Urban, Theodore Provder

By Marek W. Urban, Theodore Provder

content material: Fourier remodel IR and Raman spectroscopy of polymers : part evaluate / Peter R. Griffiths and Marek W. city --
deciding on the constitution of polyimide-metal interfaces utilizing Fourier remodel IR and Raman spectroscopy / F.J. Boerio, J.T. younger, and W.W. Zhao --
Raman microscopy and imaging of polymers / M. Claybourn, A. Luget, and K.P.J. Williams --
Multimode IR research of nylon eleven / L.J. Fina --
Rheophotoacoustic Fourier rework IR spectroscopy to check diffusion and adhesion in polymers / B.W. Ludwig, B.D. Pennington, and Marek W. city --
Step-scan Fourier rework IR reviews of polymers and liquid crystals / Richard A. Palmer, Vasilis G. Gregoriou, Akira Fuji, Eric Y. Jiang, Susan E. Plunkett, Laura M. Connors, Stephane Boccara, and James L. Chao --
comparing the weatherability of polyurethane sealants / Ralph M. Paroli, Kenneth C. Cole, and Ana H. Delgado --
Diffuse and specular reflectance measurements of polymeric fibrous fabrics / M. Papini --
tracking polymerization reactions by means of near-IR spectroscopy / Shih Ying Chang and Nam sunlight Wang --
UV-visible spectroscopy to figure out free-volume distributions in the course of multifunctional monomer polymerizations / Kristi S. Anseth, Teri A. Walker, and Christopher N. Bowman --
Multidimensional NMR spectroscopy of polymers : part assessment / Klaus Schmidt-Rohr --
Dynamics and constitution of amorphous polymers studied by way of multidimensional solid-state NMR spectroscopy / Klaus Schmidt-Rohr --
functions of ¹H-¹⁹F-¹³C triple-resonance NMR the way to the characterization of fluoropolymers / Peter L. Rinaldi, Lan Li, Dale G. Ray, III, Gerard S. Hatvany, Hsin-Ta Wang, and H. James Harwood --
Conformational sickness and its dynamics in the crystalline section of the shape II polymorph of isotactic poly(1-butene) / Haskell W. Beckham, Klaus Schmidt-Rohr, and H.W. Spiess --
NMR research of penetrant diffusion and polymer segmental movement in toluene-polyisobutylene options / Athinodoros Bandis, Paul T. Inglefield, Alan A. Jones, and Wen-Yang Wen --
Miscibility, part separation, and interdiffusion within the poly(methyl methacrylate)-poly(vinylidene fluoride) method : solid-state NMR examine / Werner E. Maas --
Oxygen absorption on fragrant polymers : ¹H NMR rest research / D. Capitani, A.L. Segre, and J. Blicharski --
Chain packing and chain dynamics of polymers with layer constructions / Hans R. Kricheldorf, Christoph Wutz, Nicolas Probst, Angelika Domschke, and Mihai Gurau --
Electron paramagnetic resonance and ¹H and ¹³C NMR examine of paper / D. Attanasio, D. Capitani, C. Federici, M. Paci, and A.L. Segre --
purposes of luminescence spectroscopy in polymer technology : part review / Ian Soutar --
Fluorescence experiences of the habit of poly(dimethylacrylamide) in dilute aqueous answer and on the solid-liquid interface / Ian Soutar, Linda Swanson, S.J.L. Wallace, K.P. Ghiggino, D.J. Haines, and T.A. Smith --
Fluorescence experiences of pyrene-labeled, water-soluble polymeric surfactants / Michael C. Kramer, Jamie R. Steger, and Charles L. McCormick --
Luminescence spectroscopic experiences of water-soluble polymers / Ian Soutar and Linda Swanson --
Photophysical examine of skinny movies of polystyrene and poly(methyl methacrylate) / E.H. Ellison and J.K. Thomas --
Photophysical techniques to characterization of visitor websites and dimension of diffusion charges to and from them in unstretched and stretched low-density polyethylene movies / Jawad Naciri, Zhiqiang Hé, Roseann M. Costantino, Liangde Lu, George S. Hammond, and Richard G. Weiss --
Photophysical habit of phenylene-vinylene polymers as studied via polarized fluorescence spectroscopy / M. Hennecke and T. Damerau --
Free-volume gap distribution of polymers probed by means of positron annihilation spectroscopy / J. Liu, Q. Deng, H. Shi, and Y.C. Jean --
tracking measure of treatment and coating thickness of photocurable resins utilizing fluorescence probe options / J.C. track and D.C. Neckers --
Spectroscopic characterization of unimer micelles of hydrophobically converted polysulfonates / Yotaro Morishima --
Fourier rework IR and NMR observations of crystalline polymer inclusion compounds / N. Vasanthan, I.D. Shin, and A.E. Tonelli --
Solvent-induced adjustments within the glass transition temperature of ethylene-vinyl alcohol copolymer studied utilizing Fourier rework IR and dynamic mechanical spectroscopy / Marsha A. Samus and Giuseppe Rossi --
Photophysical and rheological experiences of amphiphilic polyelectrolytes : correlation of polymer microstructure with associative-thickening habit / Kelly D. Branham and Charles L. McCormick --
Fourier rework IR and fluorescence spectroscopy of hugely ordered practical polymer Langmuir-Blodgett motion pictures / Tokuji Miyashita.

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Additional resources for Multidimensional Spectroscopy of Polymers. Vibrational, NMR, and Fluorescence Techniques

Example text

3. CLAYBOURN ET AL. ch003 Conclusions The discussion presented above illustrates the applications currently accessible with a commercial Raman system optimised for microprobe and imaging capabilities. Comparison is made with an FT-Raman microscope system which is clearly not sufficiently sensitive to provide any sort of routine applications with a reasonable signal/noise. Consequently, the work has focused on the applications generated using the Renishaw Raman system which can give high quality spectra on the micron dimension within a few minutes.

CLAYBOURN 1100 1200 1300 Raman wavenumbers / cm" I 1400 1500 Figure 11 - Raman spectra obtained from the top surface of the 2μιη polyethylene film on the polypropylene plaque obtained as in Figure 10 but using the lOOx microscope objective and (a) with 4 pixels height on the CCD and (b)36 pixels height on the CCD. ; ACS Symposium Series; American Chemical Society: Washington, DC, 1995. ch003 56 MULTIDIMENSIONAL SPECTROSCOPY OF POLYMERS [TIO2] ΓΠ0 ] (au) (au) 2 ο 400 300 200 500 100 300 microns microns Figure 12 - Raman map for the region around a large white inclusion found in a clear styrenated-acrylic copolymer film.

Currently, for this type of system, a collection efficiency for the Raman scatter of >25% can now be achieved (19); this is compared to <1% for the earlier Raman microscope systems. The improvement in sensitivity gives the advantages of much shorter acquisition times and allows the use of much lower laser powers, hence reducing the potential effect of sample damage under the laser beam. With the CCD detector operating in a two dimensional mode, the Raman microscope system can be used for imaging allowing the spatial distribution of a specific molecular species to be defined.

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