By Richard Hoogenboom, Ulrich S. Schubert, Frank Wiesbrock
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Extra resources for Microwave-assisted Polymer Synthesis
In another example, by careful optimization of the catalyst system it is possible to perform Heck reactions between ethene and aryl halides to generate styrenes . In the case of carbonylation reactions, molybdenum hexacarbonyl, Mo(CO)6, can be used as a carbon monoxide source. The organometallic complex starts to dissociate at temperatures around 150 C and a range of palladium-catalyzed carbonylation reactions have been performed, the most common of which are three-component couplings involving carbon monoxide, an aryl-, benzyl- or vinyl halide (or pseudohalide) and a suitable nucleophile (for a review, see ).
Energy Fuels 22:643–645 118. Leadbeater NE, Barnard TM, Stencel LM (2008) Batch and continuous-flow preparation of biodiesel derived from butanol and facilitated by microwave heating. Energy Fuels 22:2005–2008 119. Baghbanzadeh M, Kappe CO (2009) Can molecular sieves be used as water scavengers in microwave chemistry? Aust J Chem 62:244–249 120. Altman E, Stefanidis GD, van Gerven T, Stankiewicz A (2010) Process intensification of reactive distillation for the synthesis of n-propyl propionate: the effects of microwave radiation on molecular separation and esterification reaction.
Tetrahedron 64:9044–9051 72. Cheshev P, Marra A, Dondoni A (2006) First synthesis of 1,2,3-triazolo-linked (1,6)-α-D-oligomannoses (triazolomannoses) by iterative Cu(I)-catalyzed alkyne–azide cycloaddition. Org Biomol Chem 4:3225–3227 73. Joosten JAF, Tholen NTH, Maate FAE, Brouwer AJ, van Esse GW, Rijkers DTS, Liskamp RMJ, Pieters RJ (2005) High-yielding microwave-assisted synthesis of triazole-linked glycodendrimers by copper-catalyzed [3+2] cycloaddition. Eur J Org Chem 3182–3185 74. Poon CK, Chapman R, Jolliffe KA, Perrier S (2012) Pushing the limits of copper mediated azide–alkyne cycloaddition (CuAAC) to conjugate polymeric chains to cyclic peptides.